HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Chloro-2-methylpropyl)morpholine → 4-(3'-Morpholino-2-methylpropoxy)-3-phenyl-6-tert.butyl-5,6,7,8-tetrahydro-coumarin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Chloro-2-methylpropyl)morpholine | HCID 23334047 | — |
| Reactant | 4-Hydroxy-3-phenyl-6-tert.butyl-5,6,7,8-tetrahydro-coumarin | HCID 57229129 | — |
| Product | 4-(3'-Morpholino-2-methylpropoxy)-3-phenyl-6-tert.butyl-5,6,7,8-tetrahydro-coumarin | HCID 86737298 | — |
Reaction Steps
Prepared according to the method of Example 9 from 12.8 g. (0.043 mol) of 4-hydroxy-3-phenyl-6-tert.butyl-5,6,7,8-tetrahydro-coumarin and 10.7 g. (0.061 mol) of 3-morpholino-2-methyl-1-chloropropane. The product is a thick oil which cannot be crystallised.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-06a6d6ec6d294c1e84350f8d517dd94b |
| Source note | uspto-grants-1980_10 |