HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-(3-Chloro-2-methylpropyl)morpholine → 3,8-Diphenyl-4-(3'-morpholino-2'-methylpropoxy)-5,6,7,8-tetrahydrocoumarin
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-(3-Chloro-2-methylpropyl)morpholine | HCID 23334047 | — |
| Reactant | 3,8-Diphenyl-4-hydroxy-5,6,7,8-tetrahydrocoumarin | HCID 54721331 | — |
| Product | 3,8-Diphenyl-4-(3'-morpholino-2'-methylpropoxy)-5,6,7,8-tetrahydrocoumarin | HCID 23334029 | 35% |
Reaction Steps
Prepared according to the method of Example 9 from 3,8-diphenyl-4-hydroxy-5,6,7,8-tetrahydrocoumarin and 1-chloro-2-methyl-3-morpholino-propane. A thick, brown oil is obtained which cannot be crystallised. Yield 35%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04230850 |
| Source dataset | uspto-grants-1980_10 |
| ORD ID | ord-0d3ea203e0764e4f96f0b412e4d683a7 |
| Source note | uspto-grants-1980_10 |