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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 904491Generated: October 29, 2026

Glycerol → HCID 54219665, compound

https://huagongshe.com/reaction/904491

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlycerolHCID 753—
Reactantp-Toluenesulfonic acidHCID 6101—
ReactantHCID 54481030HCID 54481030—
ProductHCID 54219665HCID 54219665—

Reaction Steps

A mixture of 2.25 g. of methyl 4-(4-tetradecenylamino)benzoate, 280 mg. of glycerol, and 1.37 g. of p-toluenesulfonic acid is heated at 180° C. for 18 hours and then is partitioned between ether and 3% aqueous sodium carbonate solution. The ether layer is separated, dried, and evaporated to yield the product as a white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04230878
Source datasetuspto-grants-1980_10
ORD IDord-f019ec76298a4516a3a58f0dbf2d1c80
Source noteuspto-grants-1980_10