Sodium Hydroxide → HCID 54413875, compound

Participants

Reaction Steps

A mixture of 26.4 g. of ethyl N-[4-(4-pentadecenylamino)benzoyl]glycinate, 110 ml. of 1 N sodium hydroxide solution, and 100 ml. of ethanol is stirred at ambient temperature for 2 hours and then partially evaporated. The gaseous solution is washed with diethyl ether, acidified with 6 N hydrochloric acid, and filtered. The white solid is dried in vacuo and recrystallized from acetone.

Provenance & Evidence