HuagongsheHuagongshe Chemistry Print Report · For research reference only
Amino 4-methylbenzene-1-sulfonate → 2-Amino-1-(4-chlorobenzoyl)-isoquinolinium-p-toluene sulfonate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Amino 4-methylbenzene-1-sulfonate | HCID 10965249 | — |
| Reactant | 1-(4-Chlorobenzoyl)-isoquinoline | HCID 12243105 | — |
| Product | 2-Amino-1-(4-chlorobenzoyl)-isoquinolinium-p-toluene sulfonate | HCID 23311140 | 88.5% |
Reaction Steps
The 1-(4-chlorobenzoyl)-isoquinoline prepared as described above is reacted with O-(p-toluenesulfonyl)-hydroxylamine as described in paragraph 3 of Example 1. The 2-amino-1-(4-chlorobenzoyl)-isoquinolinium-p-toluene sulfonate is obtained with a yield of 88.5%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419355 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-d7853b3a68ae43c2a76686db6d727919 |
| Source note | uspto-grants-1983_12 |