HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 178507192, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 178522647 | HCID 178522647 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 178507192 | HCID 178507192 | — |
Reaction Steps
Hydrogenation of 10 g of 4,5-methylenedioxy-2-nitro-N-(1H-tetrazol-5-yl)benzamide in 40 ml of aqueous 1N sodium hydroxide solution and 160 ml of water and using 1 g of 10% Pd/C gave 2-amino-4,5-methylenedioxy-N-(1H-tetrazol-5-yl)benzamide as brown needles melting at about 255° C. (dec) after recrystallization from a mixture of dimethylformamide and water.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419357 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-125dca14cf9145c8936fbc132b17a9af |
| Source note | uspto-grants-1983_12 |