HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl orthoformate → HCID 178488824, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl orthoformate | HCID 31214 | — |
| Reactant | HCID 178490498 | HCID 178490498 | — |
| Product | HCID 178488824 | HCID 178488824 | — |
Reaction Steps
A suspension of 5.3 g of 2-amino-3-methoxy-N-(1H-tetrazol-5-yl)benzamide in 30 ml of triethoxymethane was refluxed for 14 hours to give 8-methoxy-3-(1H-tetrazol-5-yl)-4(3H)-quinazolinone melting at about 260°-261° C. (dec) after recrystallization from dimethylformamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419357 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-bf8aa0e678ae4012b4853ae7fee5e0da |
| Source note | uspto-grants-1983_12 |