HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 150640, compound → 6-chloro-4-oxo-10-propyl-4H-pyrano(3,2-g)quinoline-2,8-dicarboxylate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 150640 | HCID 150640 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Solvent | Water | HCID 962 | — |
| Product | 6-chloro-4-oxo-10-propyl-4H-pyrano(3,2-g)quinoline-2,8-dicarboxylate | HCID 3036586 | 85.1% |
Reaction Steps
6-Chloro-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2,8-dicarboxylic acid (0.629 g) suspended in water was treated with sodium bicarbonate (0.292 g) and stirred until complete dissolution occurred. The solution was filtered then treated with acetone. The precipitated product was collected by filtration and dried to give (0.6 g) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419352 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-80634630f281496f824dae5bc16c3208 |
| Source note | uspto-grants-1983_12 |