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HRID904665

反应详情

EQUATION

反应方程式

HRID 904665 的结构方程式

REACTANTS

反应物

2
结构：CCCc1c2nc(C(=O)O)cc(Cl)c2cc2c(=O)cc(C(=O)O)oc12
HCID150640

未命名化合物

结构：O=C([O-])O.[Na+]
HCID516892

Sodium Bicarbonate

CHNaO3

PRODUCTS

生成物

1
结构：CCCc1c2nc(C(=O)[O-])cc(Cl)c2cc2c(=O)cc(C(=O)[O-])oc12.[Na+].[Na+]
HCID3036586

Disodium 6-chloro-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2,8-dicarboxylate

C17H10ClNNa2O6

收率 85.1%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：O
溶剂HCID962

Water

H2O

PROCEDURE

实验过程

6-Chloro-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2,8-dicarboxylic acid (0.629 g) suspended in water was treated with sodium bicarbonate (0.292 g) and stirred until complete dissolution occurred. The solution was filtered then treated with acetone. The precipitated product was collected by filtration and dried to give (0.6 g) of the title compound.

WORKUP

后处理

  1. filtrationThe solution was filtered
  2. additionthen treated with acetone
  3. filtrationThe precipitated product was collected by filtration
  4. customdried