Sodium Bicarbonate → HCID 13543952, compound

HRID 904666Notes

Reaction equation

HRID 904666 reaction equation
[CH3:1][O:2][C:3]1[C:12]2[C:7](=[C:8]([CH2:21][CH2:22][CH3:23])[C:9]3[O:16][C:15]([C:17]([OH:19])=[O:18])=[CH:14][C:13](=[O:20])[C:10]=3[CH:11]=2)[N:6]=[C:5]([C:24]([OH:26])=[O:25])[CH:4]=1.C(=O)(O)[O-].[Na+:31]>O>[CH3:1][O:2][C:3]1[C:12]2[C:7](=[C:8]([CH2:21][CH2:22][CH3:23])[C:9]3[O:16][C:15]([C:17]([O-:19])=[O:18])=[CH:14][C:13](=[O:20])[C:10]=3[CH:11]=2)[N:6]=[C:5]([C:24]([O-:26])=[O:25])[CH:4]=1.[Na+:31].[Na+:31]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 13543953HCID 13543953, compound

Product 1

HCID 13543952HCID 13543952, compoundYield 92.8%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The product of step (b) (0.408 g) was dissolved in water (80 mls) containing sodium bicarbonate (0.192 g). The solution was filtered, and the filtrate freeze dried to give 0.425 g of the title product.

Workup

  1. filtrationThe solution was filtered
  2. customthe filtrate freeze dried

Sources & evidence

ORD record
ord-79d1cbf9a3f24a1dafcf2645a573dde9
Source dataset
uspto-grants-1983_12
Patent number
US04419352

Reaction notes

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