Sodium Bicarbonate → HCID 13543950, compound

Participants

Reaction Steps

The product of step (c), (2.166 g, 5.22 mmole), was added slowly to a solution of sodium bicarbonate, (0.876 g, 10.44 mmole), in water (35 ml). The resulting solution was filtered and the filtrate was freeze-dried to give the required salt as a brown solid, (2.23 g) 93%. The NMR spectrum was consistent with the required structure.

Provenance & Evidence