Sodium Bicarbonate → HCID 13543941, compound

HRID 904689Notes

Reaction equation

HRID 904689 reaction equation
[O:1]=[C:2]1[C:7]2[CH:8]=[C:9]3[C:14](=[C:15]([CH2:16][CH2:17][CH3:18])[C:6]=2[O:5][C:4]([C:22]([OH:24])=[O:23])=[CH:3]1)[N:13]=[C:12]([C:19]([OH:21])=[O:20])[CH:11]=[CH:10]3.C(=O)(O)[O-].[Na+:29]>O>[O:1]=[C:2]1[C:7]2[CH:8]=[C:9]3[C:14](=[C:15]([CH2:16][CH2:17][CH3:18])[C:6]=2[O:5][C:4]([C:22]([O-:24])=[O:23])=[CH:3]1)[N:13]=[C:12]([C:19]([O-:21])=[O:20])[CH:11]=[CH:10]3.[Na+:29].[Na+:29]

Participants

4

Reactant 2

HCID 516892Sodium BicarbonateHCID 13543942HCID 13543942, compound

Product 1

HCID 13543941HCID 13543941, compoundYield 94.7%

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

The product of step (c) (hemihydrate 0.629 g) and sodium bicarbonate (0.3145 g) were stirred in water (70 mls) until a complete solution was formed. The solution was filtered and the filtrate freeze dried to give 0.658 g of the desired salt.

Workup

  1. customwas formed
  2. filtrationThe solution was filtered
  3. customthe filtrate freeze dried

Sources & evidence

ORD record
ord-195b2d2302b94596a3526238f0772f9c
Source dataset
uspto-grants-1983_12
Patent number
US04419352

Reaction notes

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