HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenol → HCID 135773210, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenol | HCID 996 | — |
| Reactant | Potassium Hydroxide | HCID 14797 | — |
| Reactant | HCID 136035444 | HCID 136035444 | — |
| Product | HCID 135773210 | HCID 135773210 | — |
Reaction Steps
Phenol (10.0 g) which had been crushed in a mortar and pestle, was added to crushed potassium hydroxide (0.36 g) in a flask which was immersed in an oil bath. This was stirred at 60°-65° C. for 5 minutes before methyl 6-acetyl-4-chloro-7-hydroxy-8-propyl-quinoline-2-carboxylate (1.0 g) was added. The whole was stirred at 60°-65° C. for 1.5 hours and the phenol was then removed by steam distillation.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419352 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-9d86b9035c24482596c19d5a97342592 |
| Source note | uspto-grants-1983_12 |