HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Chloro-8-formyl-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2-carboxylic acid → Hydrochloric Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Chloro-8-formyl-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2-carboxylic acid | HCID 20478388 | — |
| Reactant | Jones' reagent | HCID 131709961 | — |
| Solvent | Acetone | HCID 180 | — |
| Solvent | Sodium Chloride | HCID 5234 | — |
| Product | Hydrochloric Acid | HCID 313 | — |
| Product | HCID 150640 | HCID 150640 | — |
Reaction Steps
6-Chloro-8-formyl-4-oxo-10-propyl-4H-pyrano[3,2-g]quinoline-2-carboxylic acid (0.23 g) in acetone (20 ml) was treated with Jones reagent (0.8 ml), left 20 min. at 0°, then diluted with saturated aqueous sodium chloride, and extracted with 10% sodium bicarbonate. Acidification with 2 N-hydrochloric acid gave the title compound, (200 mg), mp 340° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419352 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-23600d1eea0a442896c8550237e26359 |
| Source note | uspto-grants-1983_12 |