HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ammonium → 3-Phenylpyrrolidine-2,5-dione
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ammonium | HCID 223 | — |
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Phenylsuccinic Anhydride | HCID 136911 | — |
| Product | 3-Phenylpyrrolidine-2,5-dione | HCID 568890 | — |
Reaction Steps
10 g of phenylsuccinic anhydride was gradually added to 20 ml of 28% aqueous ammonium solution and the mixture was stirred for about 1 hour. To the reaction mixture was added aqueous hydrochloric acid solution so as to neutralize. After cooling, crystals thus formed were collected by filtration to obtain about 8.2 g of 3-phenylsuccinimide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419443 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-bf1f87100fec4ba190b33c453698846e |
| Source note | uspto-grants-1983_12 |