HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phenyl Isothiocyanate → SBB042385
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phenyl Isothiocyanate | HCID 7673 | — |
| Reactant | 2-Pyridinemethanamine | HCID 19509 | — |
| Solvent | Benzene | HCID 241 | — |
| Product | SBB042385 | HCID 737300 | 80% |
Reaction Steps
N-Phenyl-N'-2-pyridinylmethylthiourea is prepared by heating 19.8 g (0.147 m) phenylisothiocyanate and 13.2 g (0.122 m) 2-aminomethylpyridine in 500 ml benzene for 3 hr. The solid (22.8 g, 77% yield) which is collected with a melting point of 98°-9° C. and is analytically pure.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04419516 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-ad4ce3ddb61e48e3aecc53e21b159ec5 |
| Source note | uspto-grants-1983_12 |