HuagongsheHuagongshe Chemistry Print Report · For research reference only
Formaldehyde → ST4016777
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Formaldehyde | HCID 712 | — |
| Reactant | Morpholine | HCID 8083 | — |
| Reactant | Diethylphosphite | HCID 3780918 | — |
| Product | ST4016777 | HCID 520307 | — |
Reaction Steps
To a stirred mixture of morpholine (43.5 g:0.5 mole) and diethyl phosphite (69 g:0.5 mole) was added aqueous formaldehyde (41 g:0.5 mole) during 60 min. at 50°-60°. After stirring for an additional 1 hr. water was removed in vacuo and the resulting oil distilled. Pure diethyl morpholinomethylphosphonate, 105 g (87%) bp 108°-9°/0.1 mm was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04420399 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-f3924a1eee784d38b9d406f98985c373 |
| Source note | uspto-grants-1983_12 |