Ethyl benzoate → HCID 70586782, compound

HRID 904884Notes

Reaction equation

HRID 904884 reaction equation
[C:1]([O:9][CH2:10][CH3:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Al+3:12].[Cl-:13].[Cl-].[Cl-]>CCCCCC>[C:1]([O:9][CH2:10][CH3:11])(=[O:8])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[Al+3:12].[Cl-:13].[Cl-:13].[Cl-:13]

Participants

4

Reactant 2

HCID 7165Ethyl benzoateHCID 6451240Aluminum(III) Chloride

Product 1

HCID 70586782HCID 70586782, compound

Reagents, catalysts & solvents 1

HCID 8058HexaneSolvent

Conditions

Temperature
68 °C

Procedure

Ethyl benzoate (0.1 mol) and AlCl3 (anhydrous) (0.1 mol) were added to n-hexane (100 ml), followed by heating the mixture at 68° C. for 30 minutes, cooling, filtering off, washing with n-hexane and drying to obtain a reaction product (G) of ethyl benzoate--AlCl3 (1:1).

Workup

  1. temperaturecooling
  2. filtrationfiltering off
  3. washwashing with n-hexane
  4. customdrying

Sources & evidence

ORD record
ord-5cd032405cc747749d1aaa52cb9d7d43
Source dataset
uspto-grants-1983_12
Patent number
US04420593

Reaction notes

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