Dipropylamine → HCID 13565193, compound
Reaction equation
[O:1]([C:8]1[CH:9]=[C:10]([CH:13]=[CH:14][CH:15]=1)[CH:11]=O)[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.[CH2:16]([NH:19][CH2:20][CH2:21][CH3:22])[CH2:17][CH3:18].[C-:23]#[N:24].[Na+]>>[CH2:16]([N:19]([CH2:20][CH2:21][CH3:22])[CH:11]([C:10]1[CH:13]=[CH:14][CH:15]=[C:8]([O:1][C:2]2[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=2)[CH:9]=1)[C:23]#[N:24])[CH2:17][CH3:18]Participants
4
Procedure
α-(Di-n-propylamino)-3-phenoxybenzeneacetonitrile (2) was prepared from 3-phenoxybenzaldehyde, di-n-propylamine and sodium cyanide following essentially the same procedure as that described in Example 1. The product was isolated as a golden oil.
Workup
- customThe product was isolated as a golden oil
Sources & evidence
- ORD record
- ord-a2f212644d914c5caa321d6de8d13ea8
- Source dataset
- uspto-grants-1983_12
- Patent number
- US04420614
Reaction notes
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