Dimethyl Sulfate → HCID 13565196, compound

Participants

Reaction Conditions

Reaction Steps

A mixture of α-(N-isobutyl-N-methylamino)-3-phenoxybenzeneacetonitrile (7.35 g) and dimethyl sulfate (3.15 g) was stirred at a temperature of 100° C. for a period of 4 hours to give N-(α-cyano-3-phenoxybenzyl)-N-isobutyl-N,N-dimethylammonium methyl sulfate. Proton nuclear magnetic resonance spectrum (d6 -acetone; δ in ppm): 1.18 (6H, d of d); 3.45 (3H, s); 3.53 (3H, s); 6.84 (1H, s); 7.0-7.7 (9H, m).

Provenance & Evidence