HRID904952

反应详情

EQUATION

反应方程式

REACTANTS

反应物

结构：CC(C)[C@H](NC(=O)[C@H](CCC(=O)OCc1ccccc1)NC(=O)OCc1ccccc1)C(=O)N[C@H](C(=O)OC(C)(C)C)[C@@H](C)OC(C)(C)C

HCID12944649

未命名化合物

PRODUCTS

生成物

结构：CC(C)[C@H](NC(=O)[C@@H](N)CCC(=O)O)C(=O)N[C@H](C(=O)OC(C)(C)C)[C@@H](C)OC(C)(C)C

HCID131713271

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

催化剂HCID23938

Palladium

溶剂HCID887

Methanol

CH4O

PROCEDURE

实验过程

The compound obtained in accordance with (B) is subjected to catalytic hydrogenation over Pd in 80 percent strength methanol. The catalyst is filtered off and the solution is evaporated to dryness in vacuo. Triturating the residue with ether leads to a compound which is pure according to chromatography.

WORKUP

后处理

filtrationThe catalyst is filtered off
customthe solution is evaporated to dryness in vacuo
customTriturating the residue with ether