HuagongsheHuagongshe Chemistry Print Report · For research reference only
Z-Glu(OBzl)-Val-Thr(But)-OBut → Glu-Val-Thr(But)-OBut
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Z-Glu(OBzl)-Val-Thr(But)-OBut | HCID 12944649 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | Glu-Val-Thr(But)-OBut | HCID 131713271 | — |
Reaction Steps
The compound obtained in accordance with (B) is subjected to catalytic hydrogenation over Pd in 80 percent strength methanol. The catalyst is filtered off and the solution is evaporated to dryness in vacuo. Triturating the residue with ether leads to a compound which is pure according to chromatography.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04420424 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-d7f4229f67f640c3915c3b9ad22c34c4 |
| Source note | uspto-grants-1983_12 |