HuagongsheHuagongshe Chemistry Print Report · For research reference only
Butyl Chloride → HCID 57110154, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Butyl Chloride | HCID 8005 | — |
| Reactant | 3-Amino-1-methyl-5-methylthio-1,2,4-triazole | HCID 522820 | — |
| Reactant | Propan-2-yl 2-[(oxomethylidene)sulfamoyl]benzoate | HCID 13305294 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57110154 | HCID 57110154 | — |
Reaction Steps
A mixture of 0.7 grams (0.00486 mole) of 3-amino-1-methyl-5-methylthio-1H-1,2,4-triazole and 4.0 grams of 2-(isopropoxycarbonyl)benzenesulfonylisocyanate was stirred in 12 ml of dry methylene chloride at ambient temperature overnight. After addition of 4 ml of 1-chlorobutane, a white solid precipitated which was filtered, washed with 1-chlorobutane and dried, yield 1.3 grams, m.p. 192°-194°.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421550 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-65b1b2576cc641acafd0d2cb4a787528 |
| Source note | uspto-grants-1983_12 |