Water → HCID 15571367, compound

Participants

Reaction Steps

Similarly, 1.0 g of the above-mentioned enamine type adduct compound, that is, 5-(3,4-methylenedioxyphenyl)-2-[3-(3,4-methylenedioxyphenyl)-1-morpholinoallylidene]-cyclohexane-1,3-dione, was dissolved in 80 ml of acetic acid, and 0.5 g of a 5% palladium-carbon catalyst and 30 ml of deionized water were added to the solution and catalytic reduction was carried out with hydrogen under atmospheric pressure for 4 hours to obtain 0.38 g (the yield being 44%) of the desired compound.

Provenance & Evidence