Hydrochloric Acid → HCID 15916372, compound

Participants

Reaction Steps

A saturated solution of dry hydrogen chloride in dry ether (10 ml) is added to 1-fluoro-2,5-di-(N-tert.butoxycarbonylamino)-6-heptyne obtained as in Step D above (1 mmole) and left overnight at room temperature. The dichlorohydride which forms as crystals is filtered, washed with ether, and dried to give the title compound (0.21 g).

Provenance & Evidence