HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → HCID 54471508, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Sodium hydride | HCID 24758 | — |
| Reactant | HCID 53994231 | HCID 53994231 | — |
| Solvent | Dimethylformamide | HCID 6228 | — |
| Product | HCID 54471508 | HCID 54471508 | 69% |
Reaction Steps
As in Example 1(b), 16 mg of imidazole, 10 mg of 55% sodium hydride and 70 mg of cis-6-(2,4-dichlorobenzyloxy)-2-tosyloxymethyltetrahydropyran were reacted in dimethylformamide, to give 37 mg of the title compound in the form of a colourless oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04421758 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-6d510b5e615f4deca004a9d2a812b55a |
| Source note | uspto-grants-1983_12 |