huagongshe.com
HRID905057

反应详情

EQUATION

反应方程式

HRID 905057 的结构方程式

REACTANTS

反应物

3
结构：c1c[nH]cn1
HCID795

Imidazole

C3H4N2

结构：[H-].[Na+]
HCID24758

Sodium hydride

HNa

结构：Cc1ccc(S(=O)(=O)OC[C@H]2CCC[C@@H](OCc3ccc(Cl)cc3Cl)O2)cc1
HCID53994231

未命名化合物

PRODUCTS

生成物

1
结构：Clc1ccc(CO[C@@H]2CCC[C@H](Cn3ccnc3)O2)c(Cl)c1
HCID54471508

未命名化合物

收率 69%

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CN(C)C=O
溶剂HCID6228

Dimethylformamide

C3H7NO

PROCEDURE

实验过程

As in Example 1(b), 16 mg of imidazole, 10 mg of 55% sodium hydride and 70 mg of cis-6-(2,4-dichlorobenzyloxy)-2-tosyloxymethyltetrahydropyran were reacted in dimethylformamide, to give 37 mg of the title compound in the form of a colourless oil.