Ethanol → HCID 3067727, compound

Participants

Reaction Steps

Then, the above product was dissolved in 300 ml of ethanol, to which were added 15.64 parts of hydroxylamine hydrochloride and 17.8 parts of pyridine, and the reaction was effected under reflux for 1.5 hours. Thereafter, the product was treated as in Example 1 to obtain 20.4 parts of 6-chloro-4-oximino-1-acetyl-1,2,3,4-tetrahydroquinoline as white crystals.

Provenance & Evidence