Benzaldehyde → HCID 3068101, compound

HRID 905130Notes

Reaction equation

HRID 905130 reaction equation
[C:1]([C:4]1[CH:5]=[CH:6][C:7]([O:15][CH3:16])=[C:8]([CH:10]=[CH:11][C:12]([OH:14])=[O:13])[CH:9]=1)(=[O:3])[CH3:2].[CH:17](=O)[C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1>[OH-].[Na+]>[C:1]([C:4]1[CH:5]=[CH:6][C:7]([O:15][CH3:16])=[C:8]([CH:10]=[CH:11][C:12]([OH:14])=[O:13])[CH:9]=1)(=[O:3])[CH:2]=[CH:17][C:18]1[CH:23]=[CH:22][CH:21]=[CH:20][CH:19]=1

Participants

4

Reactant 2

HCID 240BenzaldehydeHCID 53684458HCID 53684458, compound

Product 1

HCID 3068101HCID 3068101, compound

Reagents, catalysts & solvents 1

HCID 14798Sodium HydroxideSolvent

Procedure

Using 10 g (0.045 mole) of the acid obtained in step (c), 80 ml of 20% sodium hydroxide and 5 g (0.045 mole) of benzaldehyde and according to a modus operandi similar to the one described in step (c) of preparation I, 11.5 g of the desired pure product are obtained, m.p.=204° C.

Workup

  1. customdescribed in step (c) of preparation I, 11.5 g of the desired pure product
  2. customare obtained

Sources & evidence

ORD record
ord-343dee5c32ae4a769ce89680a49fab32
Source dataset
uspto-grants-1983_12
Patent number
US04421927

Reaction notes

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