HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 13014243, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | Glycine, N-(2,6-diethylphenyl)-, ethyl ester | HCID 170107 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 13014243 | HCID 13014243 | — |
Reaction Steps
58.7 g (0.25 mol) of 2,6-diethyl-anilino-acetic acid ethyl ester and 25 g of hydrazine hydrate were left to stand in 200 ml of ethanol for 24 hours. Thereafter, the mixture was concentrated by distilling off the solvent and the residue was extracted by stirring with water. After drying, 50.5 g (91% of theory) of colorless crystals of 2,6-diethyl-anilino-acetic acid hydrazide of melting point 71° to 73° C. were obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04422866 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-c9da13cbc97e45b280ec8b19510975b9 |
| Source note | uspto-grants-1983_12 |