Potassium Carbonate → HCID 12698923, compound

HRID 905208Notes

Reaction equation

HRID 905208 reaction equation
Cl.[CH3:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:14])[CH:7]=[CH:6]2.C(=O)([O-])[O-].[K+].[K+]>CCOCC>[CH3:2][C:3]1[CH:4]=[C:5]2[C:10](=[CH:11][CH:12]=1)[CH:9]=[C:8]([C:13]([CH2:15][N:16]1[CH:20]=[CH:19][N:18]=[CH:17]1)=[O:14])[CH:7]=[CH:6]2

Participants

4

Reactant 2

HCID 11430Potassium CarbonateHCID 12698924HCID 12698924, compound

Product 1

HCID 12698923HCID 12698923, compound

Reagents, catalysts & solvents 1

HCID 3283Diethyl EtherSolvent

Procedure

1-[(6-Methyl-2-naphthoyl)methyl]imidazole hydrochloride (1.0 g.) suspended in 50 ml. of ether is stirred with excess dilute aqueous potassium carbonate solution until the salt is completely dissolved. The organic layer is then separated, washed twice with water, dried over magnesium sulfate and evaporated to yield 1-[(6-methyl-2-naphthoyl)methyl]imidazole.

Workup

  1. dissolutionis completely dissolved
  2. customThe organic layer is then separated
  3. washwashed twice with water
  4. dry with materialdried over magnesium sulfate
  5. customevaporated

Sources & evidence

ORD record
ord-c6f684f0e78545d7b74e49bab5dd45ce
Source dataset
uspto-grants-1983_12
Patent number
US04423057

Reaction notes

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