HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophenol → HCID 14320983, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophenol | HCID 7969 | — |
| Reactant | 5-Bromo-2-chloropyrimidine | HCID 606665 | — |
| Product | HCID 14320983 | HCID 14320983 | — |
Reaction Steps
The title compound was prepared from 2-chloro-5-bromo-pyrimidine and thiophenol as described in Example 1; yield: 90% of a non-crystalline product which was pure enough for the successive oxidation. MS m/e: 267 (M, 100%). 1H NMR (CDCl3): δ7.4 (Ph), 8.50 (H-4, H-6).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04423047 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-4b855e48ad724771a974ea21fa1c8e96 |
| Source note | uspto-grants-1983_12 |