HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Carbonate → N-[2-(benzylamino)ethyl]-2-phenylacetamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Carbonate | HCID 10340 | — |
| Reactant | HCID 20446801 | HCID 20446801 | — |
| Solvent | Water | HCID 962 | — |
| Product | N-[2-(benzylamino)ethyl]-2-phenylacetamide | HCID 12876177 | — |
Reaction Steps
The free base was liberated from the hydrochloride (15 g.) by basification of a solution in water (150 ml.) with solid sodium carbonate. The aqueous mixture was extracted with ethyl acetate (3×100 ml.) and the extracts were dried (MgSO4) and evaporated to give N-[2-(benzylamino)ethyl]-2-phenylacetamide as an oil (13.0 g.), which slowly crystallised.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04423070 |
| Source dataset | uspto-grants-1983_12 |
| ORD ID | ord-d9c9257511134eb4b3038dac4b0a4ade |
| Source note | uspto-grants-1983_12 |