Acrylonitrile → Propanenitrile, 3-[2-(dimethylamino)ethoxy]-

HRID 905319Notes

Reaction equation

HRID 905319 reaction equation
[C:1](#[N:4])[CH:2]=[CH2:3].[CH3:5][N:6]([CH2:8][CH2:9][OH:10])[CH3:7].[Na]>>[C:1]([CH2:2][CH2:3][O:10][CH2:9][CH2:8][N:6]([CH3:7])[CH3:5])#[N:4]

Participants

4

Reactant 3

HCID 7855AcrylonitrileHCID 79022-(Dimethylamino)ethanolHCID 5360545Sodium

Product 1

HCID 89692Propanenitrile, 3-[2-(dimethylamino)ethoxy]-

Procedure

530 g of acrylonitrile are added dropwise to 890 g (10 mols) of dimethylaminoethanol and 0.3 g of dissolved sodium at room temperature. The mixture is left to stand for 24 hours and low-boiling constituents are distilled off.

Workup

  1. waitThe mixture is left
  2. distillationlow-boiling constituents are distilled off

Sources & evidence

ORD record
ord-c0f92b1c26154dc29e6f93931ae5d1cd
Source dataset
uspto-grants-1983_12
Patent number
US04423194

Reaction notes

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