Urea → HCID 131729135, compound

HRID 905495Notes

Reaction equation

HRID 905495 reaction equation
Cl.[NH2:2][N+:3]([NH2:7])=[C:4]([NH2:6])[NH2:5].[NH2:8][C:9]([NH2:11])=[O:10]>>[NH2:2][N+:3]([NH2:7])=[C:4]([NH2:6])[NH2:5].[NH2:8][C:9]([NH2:11])=[O:10]

Participants

3

Reactant 2

HCID 1176UreaHCID 22595028HCID 22595028, compound

Product 1

HCID 131729135HCID 131729135, compound

Conditions

Temperature
10 °C

Procedure

Diaminoguanidinium hydrochloride (13.0 g, 103.5 mmol) and urea (12.4 g, 207.1 mmol) were placed in a flask with stirring. The flask was heated to 10° C. and stirred until a melt was formed, at which time the mixture was cooled to room temperature and the product collected as a white solid.

Workup

  1. stirringstirred until a melt
  2. customwas formed, at which time the mixture
  3. temperaturewas cooled to room temperature
  4. customthe product collected as a white solid

Sources & evidence

ORD record
ord-52e61f1e768a412fb85dfdb976387cab
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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