Trifluoroacetic acid → HCID 178514274, compound

HRID 905503Notes

Reaction equation

HRID 905503 reaction equation
[NH2:1][N:2]1[CH:6]=[N:5][N:4]=[CH:3]1.[F:7][C:8]([F:13])([F:12])[C:9]([OH:11])=[O:10]>O>[O-:11][C:9]([C:8]([F:13])([F:12])[F:7])=[O:10].[NH2:1][N:2]1[CH:6]=[NH+:5][N:4]=[CH:3]1

Participants

4

Reactant 2

HCID 6422Trifluoroacetic acidHCID 114324-Amino-1,2,4-triazole

Product 1

HCID 178514274HCID 178514274, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

4-Amino-1,2,4-triazole (1.27 g, 15.14 mmol) was dissolved in 5 ml of distilled water. Trifluoroacetic acid (1.12 ml, 15.14 mmol) was added via syringe at room temperature and the reaction was stirred at room temperature for 1 hour. The water was removed in vacuo with heating to approximately 90° C. for 4 hours.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours

Sources & evidence

ORD record
ord-beb52579d6ce409d896a137819b31dd2
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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