Carbon Dioxide → HCID 178514406, compound

HRID 905510Notes

Reaction equation

HRID 905510 reaction equation
[C:1]([OH:10])(=[O:9])[C@@H:2]([C@H:4]([C:6]([OH:8])=[O:7])[OH:5])[OH:3].C(=O)(O)O.[NH2:15][NH:16][C:17]([NH2:19])=[NH:18].C(=O)=O>O>[C:6]([C@@H:4]([C@H:2]([C:1]([O-:10])=[O:9])[OH:3])[OH:5])([O-:8])=[O:7].[NH2:15][NH:16][C:17]([NH2:19])=[NH2+:18].[NH2:15][NH:16][C:17]([NH2:19])=[NH2+:18]

Participants

5

Reactant 3

HCID 280Carbon DioxideHCID 444305L-Tartaric acidHCID 178513185HCID 178513185, compound

Product 1

HCID 178514406HCID 178514406, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

L-Tartaric acid (20.00 g, 133.25 mmol) was dissolved in 200 ml of distilled water. Aminoguanidine bicarbonate (36.27 g, 266.51 mmol) was added in portions at room temperature (carbon dioxide gas was evolved) and the reaction was stirred at room temperature for 24 hours. The water was removed in vacuo with heating to approximately 90° C. for 4 hours. The product was isolated as a white solid.

Workup

  1. customThe water was removed in vacuo
  2. temperaturewith heating to approximately 90° C. for 4 hours
  3. customThe product was isolated as a white solid

Sources & evidence

ORD record
ord-e2d2330f8e27459bbb0dcc04d722d945
Source dataset
uspto-grants-2011_09
Patent number
US08012277B2

Reaction notes

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