Triethylamine → HCID 57699402, compound

Participants

Reaction Steps

N-[3-(2-aminoethyl)-4-(4-morpholinophenyl)thiazol-2(3H)-ylidene]-3-fluoroaniline obtained in Example 1 was dissolved in THF, and thereto was added triethylamine, and then thereto was added 4-nitrophenyl chloroformate under ice-cooling. The mixture was stirred for 2 hours. Thereto was added ammonia water, and the mixture was stirred for 2 hours at room temperature. The resulting compound was recrystallized from methanol to give the titled compound.

Provenance & Evidence