HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 131729149, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 131729150 | HCID 131729150 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 131729149 | HCID 131729149 | — |
Reaction Steps
Racemic cis 1-(4-amino-5-methyl-azepan-1-yl)-ethanone was prepared in the same manner from racemic cis 1-(4-benzylamino-5-methyl-azepan-1-yl)-ethanone. In this instance, 1 atm H2 was used instead of 55 psi, Pd/C was used instead of Pd(OH)2/C, EtOAc was used instead of EtOH, and the HCl treatment was omitted.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08012974B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-bc9523aed4224d728a40ae13aabe13ab |
| Source note | uspto-grants-2011_09 |