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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 90605Generated: October 30, 2026

Methanol → Tert-butyl 9-amino-2,2-difluoro-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h][1]benzazepine-5-carboxylate

https://huagongshe.com/reaction/90605

Reaction equation

Participants

RoleNameHCIDCharge
ReactantMethanolHCID 887—
ReactantTolueneHCID 1140—
Reactant1,8-Diazabicyclo(5.4.0)undec-7-eneHCID 81184—
ReactantTert-butyl 2,2-difluoro-9-hydroxy-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h][1]benzazepine-5-carboxylateHCID 68679481—
ReactantHCID 90857522HCID 90857522—
ProductTert-butyl 9-amino-2,2-difluoro-6,7,8,9-tetrahydro-[1,3]dioxolo[4,5-h][1]benzazepine-5-carboxylateHCID 68679505—

Provenance & Evidence

DOI10.1039/C8SC04228D
Source datasetTraining data from https://doi.org/10.1039/C8SC04228D (2/10)
ORD IDord-6d8881ba50914ff49cd8c3bed5b9a26c
Source noteTraining data from https://doi.org/10.1039/C8SC04228D (2/10)