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HRID906190

反应详情

EQUATION

反应方程式

HRID 906190 的结构方程式

REACTANTS

反应物

3
结构：CC[C@@H](C)N
HCID2724537

(R)-sec-Butylamine

C4H11N

结构：CCOC(=O)c1cc(N[C@H](C)CC)c(C#N)cc1Br
HCID67404527

未命名化合物

结构：CCNc1cc(C#N)c(N[C@H](C)CC)cc1C(=O)OCC
HCID67405722

未命名化合物

PRODUCTS

生成物

1
结构：CCNc1cc(C(N)=O)c(N[C@H](C)CC)cc1C(=O)O
HCID57748590

未命名化合物

PROCEDURE

实验过程

Synthesized according to the method of reagent preparation 50 by using (1R)-1-methylpropylamine in step 1 then following step 2 with the conversion of ethyl 2-bromo-4-cyano-5-{[(1R)-1-methylpropyl]amino}benzoate to ethyl 4-cyano-2-(ethylamino)-5-{[(1R)-1-methylpropyl]amino}benzoate according to the method described in step 1 then proceeding through steps 3 and 4. MS (EI) for C14H21N3O3: 280 (MH+).

WORKUP

后处理

  1. customSynthesized
  2. customaccording to the method of reagent preparation 50