huagongshe.com
HRID906246

反应详情

EQUATION

反应方程式

HRID 906246 的结构方程式

REACTANTS

反应物

2
结构：O=P(Cl)(Cl)Cl
HCID24813

Phosphoric trichloride

Cl3OP

结构：O=c1nc(-c2ccc(C(F)(F)F)nc2)cc(C(F)F)[nH]1
HCID67393475

未命名化合物

PRODUCTS

生成物

1
结构：FC(F)c1cc(-c2ccc(C(F)(F)F)nc2)nc(Cl)n1
HCID86624632

未命名化合物

PROCEDURE

实验过程

The title compound was prepared from 6-difluoromethyl-4-(6-trifluoromethyl-pyridin-3-yl)-1H-pyrimidin-2-one (6.37 g, 0.022 mol) and phosphoroxychloride (34 ml) according to the general procedure I. Obtained as a brown oil (6.65 g, 98%). MS (ISP) 310.2 [(M+H)+].