HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Carbonate → HCID 67390298, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Carbonate | HCID 11125 | — |
| Reactant | 4-Fluoro-3-(trifluoromethyl)benzonitrile | HCID 144255 | — |
| Reactant | (2S,3S)-2,3-dimethylpyrrolidin-3-ol | HCID 59556870 | — |
| Product | HCID 67390298 | HCID 67390298 | — |
Reaction Steps
By an operation in the same manner as in Example 1 and using (2S,3S)-2,3-dimethylpyrrolidin-3-ol 0.5 oxalate (228 mg), 4-fluoro-3-(trifluoromethyl)benzonitrile (397 mg) and lithium carbonate (206 mg), the title compound was obtained as a colorless oil (yield: 220 mg, yield: 55%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08013008B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-a35b70ff548a4cc6814cb3c2c9a4914f |
| Source note | uspto-grants-2011_09 |