HuagongsheHuagongshe Chemistry Print Report · For research reference only
Lithium Carbonate → HCID 24986667, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Lithium Carbonate | HCID 11125 | — |
| Reactant | 2,4,6-Trifluorobenzonitrile | HCID 737177 | — |
| Reactant | (2S,3S)-2,3-dimethylpyrrolidin-3-ol | HCID 59556870 | — |
| Product | HCID 24986667 | HCID 24986667 | — |
Reaction Steps
By an operation in the same manner as in Example 1 and using (2S,3S)-2,3-dimethylpyrrolidin-3-ol 0.5 oxalate (300 mg), 2,4,6-trifluorobenzonitrile (882 mg) and lithium carbonate (276 mg), the title compound was obtained as a colorless solid (yield: 263 mg, yield: 56%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08013008B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-aeda77b977ee4840925c20ab74827a00 |
| Source note | uspto-grants-2011_09 |