HRID907060

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID581760

3-Thiopheneboronic acid

C4H5BO2S

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1cccc(Br)c1

HCID67395600

未命名化合物

PRODUCTS

生成物

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1cccc(-c2ccsc2)c1

HCID67397080

未命名化合物

收率 26%

PROCEDURE

实验过程

By carrying out the operation analogously to example 13, starting from 3-bromophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, obtained according to preparation VII, and 3-thiopheneboronic acid, the expected product is obtained in the form of white crystals with a yield of 26%.

WORKUP

后处理

customobtained