HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiophene-3-boronic acid → 3-(3-Thienyl)phenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiophene-3-boronic acid | HCID 581760 | — |
| Reactant | 3-bromophenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 67395600 | — |
| Product | 3-(3-Thienyl)phenyl 2,3,4-tri-O-acetyl-5-thio-beta-D-xylopyranoside | HCID 67397080 | 26% |
Reaction Steps
By carrying out the operation analogously to example 13, starting from 3-bromophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, obtained according to preparation VII, and 3-thiopheneboronic acid, the expected product is obtained in the form of white crystals with a yield of 26%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08013010B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-afb30c41cfdb4288a658d4366e1ca85e |
| Source note | uspto-grants-2011_09 |