HRID907068

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2736778

2-Methoxypyrimidine-5-boronic acid

C5H7BN2O3

结构：CC(=O)O[C@@H]1[C@@H](OC(C)=O)[C@H](OC(C)=O)CS[C@H]1Oc1cccc(Br)c1

HCID67395600

未命名化合物

PRODUCTS

生成物

结构：COc1ncc(-c2cccc(O[C@@H]3SC[C@@H](OC(C)=O)[C@H](OC(C)=O)[C@H]3OC(C)=O)c2)cn1

HCID67396331

未命名化合物

PROCEDURE

实验过程

By carrying out the operation analogously to example 3, starting from 3-bromophenyl 2,3,4-tri-O-acetyl-5-thio-β-D-xylopyranoside, obtained according to preparation VII, and 2-methoxy-5-pyrimidineboronic acid, the expected product is obtained and is reacted further without additional purification in order to obtain the nonacetylated xyloside.

WORKUP

后处理

customobtained