Hydrochloric Acid → HCID 131729161, compound

Participants

Reaction Steps

A solution of Example 6 step (iii) (0.2 g) in methanol (10 mL) was treated with 4.0M HCl in 1,4-dioxane (10 mL) and the solution stirred at room temperature for 2 hours. The volatiles were then removed under reduced pressure and the residue triturated with diethyl ether to give the product, after filtration as a solid (80 mg).

Provenance & Evidence