HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 131729161, compound → HCID 25020510, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 131729161 | HCID 131729161 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 25020510 | HCID 25020510 | — |
Reaction Steps
10% Pd/C (20 mg) was added to a solution of Example 7 (60 mg) in ethanol (20 mL) and the mixture subjected to hydrogenation at 3 Barr for 2 hours. The reaction mixture was filtered and evaporated under reduced pressure to give the title compound as the hydrochloride salt as a solid (50 mg).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08012979B2 |
| Source dataset | uspto-grants-2011_09 |
| ORD ID | ord-65cf78b4000d40afa82ea8981268fbf0 |
| Source note | uspto-grants-2011_09 |