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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 907352Generated: October 29, 2026

Hydrochloric Acid → HCID 57551750, compound

https://huagongshe.com/reaction/907352

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHydrochloric AcidHCID 313—
ReactantHCID 57551799HCID 57551799—
SolventMethanolHCID 887—
Solvent1,4-DioxaneHCID 31275—
ProductHCID 57551750HCID 57551750—

Reaction Steps

To a solution of the product of step i) (170 mg) in methanol (5 mL) was added 4M HCl in 1,4-dioxane (5 mL). The solution was stirred at room temperature for 2 hours. The volatiles were removed under vacuum and the residue was purified by HPLC to yield the title compound as a solid (25 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08012979B2
Source datasetuspto-grants-2011_09
ORD IDord-880b563dbf234437961835812c1e05b6
Source noteuspto-grants-2011_09